Question

Difficulty: Very hardProcedural Steps

To isolate zircon crystals from a granite sample for uranium-lead geochronology, geologists follow a rigorous multi-step physical and chemical separation protocol. First, the bulk granite is reduced to a fine powder using a jaw crusher followed by a disc mill, ensuring the grain size matches the expected size of individual zircon grains without fracturing them. Next, the resulting powder is passed through a wet-shaking Wilfley table, which uses water flow and density differentials to separate lighter quartz and feldspar from the heavier mineral fraction. Before the remaining heavy concentrate can be subjected to magnetic separation, it must be thoroughly dried in an oven. Once dry, the sample is passed through a hand magnet to extract highly magnetic magnetite, and subsequently processed through a Frantz isodynamic separator at progressively higher electrical currents to isolate weakly magnetic minerals like biotite and hornblende from non-magnetic zircon. The non-magnetic residue is then immersed in methylene iodide, a heavy liquid with a specific gravity of 3.3, allowing the denser zircons to sink while any remaining lighter minerals float to the surface. Finally, the recovered zircon fraction is hand-picked under a binocular microscope to select high-quality, inclusion-free grains for mass spectrometry.

Based on the geological sample preparation protocol described in the passage, which of the following lists two actions that must both be completed before the non-magnetic zircon can be separated from weakly magnetic minerals like biotite and hornblende?

  1. A
    Drying the heavy concentrate in an oven, and immersing the non-magnetic residue in methylene iodide.
  2. B
    Extracting magnetite using a hand magnet, and hand-picking inclusion-free grains under a microscope.
  3. Separating quartz and feldspar on a Wilfley table, and extracting magnetite using a hand magnet.Answer
  4. D
    Reducing the bulk granite to a fine powder, and floating the lighter minerals in methylene iodide.

Answer

Separating quartz and feldspar on a Wilfley table, and extracting magnetite using a hand magnet.
The correct answer is correct because both separating quartz and feldspar on a Wilfley table and extracting magnetite with a hand magnet occur before the sample is processed through the Frantz isodynamic separator to isolate the weakly magnetic minerals from the non-magnetic zircon. This matches the chronological sequence of the geological sample preparation protocol.

Step-by-Step Solution

1
Locate the target process step in the passage where non-magnetic zircon is separated from weakly magnetic minerals like biotite and hornblende.
This separation is achieved using the Frantz isodynamic separator.
Identifying the specific instrument and step helps trace the chronological boundary.
2
List all preceding steps that occur prior to the Frantz isodynamic separator processing.
The steps are: milling/crushing, separation on a Wilfley table, drying in an oven, and manual extraction of magnetite using a hand magnet.
Establishing the sequence of events guarantees that we only select prerequisite operations.
3
Evaluate the answer choices to identify the pair of actions that falls entirely within the list of preceding steps.
Separating quartz and feldspar on a Wilfley table (step 2 in sequence) and extracting magnetite using a hand magnet (step 4 in sequence) are both completed prior to the Frantz separation. Other options contain steps that occur afterward, such as methylene iodide immersion or hand-picking under a microscope.
Synthesizing the timeline of the experiment reveals which steps are prerequisites for the magnetic separation phase.

Key Concept

Understanding and tracing the sequence of procedural steps in a technical or scientific protocol.
Estimated Time:3m 0s
Rate this question