Question

Difficulty: MediumFiltration, Evaporation, and Crystallization

A chemist needs to recover solid solutes separately from two aqueous mixtures: Solution X containing sodium chloride (NaCl\text{NaCl}) to obtain anhydrous salt, and Solution Y containing hydrated iron(II) tetraoxosulfate(VI) (FeSO47H2O\text{FeSO}_4 \cdot 7\text{H}_2\text{O}) to obtain pure hydrated crystals. Which combination of techniques should be used to obtain the solutes from Solution X and Solution Y respectively?

  1. Evaporation to dryness for Solution X, and crystallization for Solution YAnswer
  2. B
    Crystallization for Solution X, and evaporation to dryness for Solution Y
  3. C
    Evaporation to dryness for both Solution X and Solution Y
  4. D
    Filtration for Solution X, and simple distillation for Solution Y

Answer

Evaporation to dryness for Solution X, and crystallization for Solution Y
The correct response identifies that sodium chloride solution can be safely evaporated to dryness because the salt is heat-stable and has no water of crystallization to preserve. Conversely, hydrated iron(II) tetraoxosulfate(VI) requires crystallization (partial evaporation to a saturated state followed by cooling) to retain its water of crystallization and avoid thermal decomposition.

Step-by-Step Solution

1
Analyze thermal stability and solute characteristics of Solution X
Sodium chloride (NaCl\text{NaCl}) is thermally stable at heating temperatures and does not rely on water of crystallization.
Evaporation to dryness completely removes the solvent water, leaving behind dry anhydrous sodium chloride.
2
Analyze thermal stability and solute characteristics of Solution Y
Hydrated iron(II) tetraoxosulfate(VI) (FeSO47H2O\text{FeSO}_4 \cdot 7\text{H}_2\text{O}) loses its water of crystallization and decomposes if heated to dryness.
Crystallization involves concentrating the solution partially and cooling it slowly so pure hydrated crystals precipitate without thermal decomposition.

Key Concept

Selecting evaporation to dryness versus crystallization based on thermal stability and water of crystallization
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